One Step Synthesis of NiO Nanoparticles via Solid-State Thermal Decomposition at Low-Temperature of Novel Aqua(2,9-dimethyl-1,10-phenanthroline)NiCl2 Complex
Identifieur interne : 000213 ( Main/Exploration ); précédent : 000212; suivant : 000214One Step Synthesis of NiO Nanoparticles via Solid-State Thermal Decomposition at Low-Temperature of Novel Aqua(2,9-dimethyl-1,10-phenanthroline)NiCl2 Complex
Auteurs : Assem Barakat ; Mousa Al-Noaimi ; Mohammed Suleiman ; Abdullah S. Aldwayyan ; Belkheir Hammouti ; Taibi Ben Hadda ; Salim F. Haddad ; Ahmed Boshaala ; Ismail WaradSource :
- International Journal of Molecular Sciences [ 1422-0067 ] ; 2013.
Abstract
[NiCl2(C14H12N2)(H2O)] complex has been synthesized from nickel chloride hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as
Url:
DOI: 10.3390/ijms141223941
PubMed: 24351867
PubMed Central: 3876087
Affiliations:
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">One Step Synthesis of NiO Nanoparticles via Solid-State Thermal Decomposition at Low-Temperature of Novel <italic>Aqua</italic>(2,9-dimethyl-1,10-phenanthroline)NiCl<sub>2</sub> Complex</title><author><name sortKey="Barakat, Assem" sort="Barakat, Assem" uniqKey="Barakat A" first="Assem" last="Barakat">Assem Barakat</name><affiliation><nlm:aff id="af1-ijms-14-23941">Department of Chemistry, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi Arabia; E-Mail:<email>ambarakat@ksu.edu.sa</email></nlm:aff></affiliation></author><author><name sortKey="Al Noaimi, Mousa" sort="Al Noaimi, Mousa" uniqKey="Al Noaimi M" first="Mousa" last="Al-Noaimi">Mousa Al-Noaimi</name><affiliation><nlm:aff id="af2-ijms-14-23941">Department of Chemistry, Hashemite University, Zarqa 13115, Jordan; E-Mail:<email>manoaimi@hu.edu.jo</email></nlm:aff></affiliation></author><author><name sortKey="Suleiman, Mohammed" sort="Suleiman, Mohammed" uniqKey="Suleiman M" first="Mohammed" last="Suleiman">Mohammed Suleiman</name><affiliation><nlm:aff id="af3-ijms-14-23941">Department of Chemistry, Science College, AN-Najah National University, P.O. Box 7, Nablus, Palestine; E-Mail:<email>suleimanshtaya@najah.edu</email></nlm:aff></affiliation></author><author><name sortKey="Aldwayyan, Abdullah S" sort="Aldwayyan, Abdullah S" uniqKey="Aldwayyan A" first="Abdullah S." last="Aldwayyan">Abdullah S. Aldwayyan</name><affiliation><nlm:aff id="af4-ijms-14-23941">Department of Physics and Astronomy, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi Arabia; E-Mail:<email>dwayyan@ksu.edu.sa</email></nlm:aff></affiliation></author><author><name sortKey="Hammouti, Belkheir" sort="Hammouti, Belkheir" uniqKey="Hammouti B" first="Belkheir" last="Hammouti">Belkheir Hammouti</name><affiliation><nlm:aff id="af5-ijms-14-23941">Laboratoire de Chimie Appliquée et Environnement, LCAE-URAC18, Faculity of Science, University Mohammed Premier, Oujda 60000, Morocco; E-Mail:<email>hammoutib@gmail.com</email></nlm:aff></affiliation></author><author><name sortKey="Ben Hadda, Taibi" sort="Ben Hadda, Taibi" uniqKey="Ben Hadda T" first="Taibi" last="Ben Hadda">Taibi Ben Hadda</name><affiliation><nlm:aff id="af6-ijms-14-23941">Lab of Chemical Material, FSO, University Mohammed Premier, Oujda 60000, Morocco; E-Mail:<email>taibi.ben.hadda@gmail.com</email></nlm:aff></affiliation></author><author><name sortKey="Haddad, Salim F" sort="Haddad, Salim F" uniqKey="Haddad S" first="Salim F." last="Haddad">Salim F. Haddad</name><affiliation><nlm:aff id="af7-ijms-14-23941">Department of Chemistry, the University of Jordan, Amman 11942, Jordan; E-Mail:<email>hadsal2003@yahoo.com</email></nlm:aff></affiliation></author><author><name sortKey="Boshaala, Ahmed" sort="Boshaala, Ahmed" uniqKey="Boshaala A" first="Ahmed" last="Boshaala">Ahmed Boshaala</name><affiliation><nlm:aff id="af8-ijms-14-23941">Department of Chemistry, Faculty of Science, Benghazi University, P.O. Box 1308, Benghazi 5341, Libya; E-Mail:<email>ahmedboshaala@yahoo.co.uk</email></nlm:aff></affiliation></author><author><name sortKey="Warad, Ismail" sort="Warad, Ismail" uniqKey="Warad I" first="Ismail" last="Warad">Ismail Warad</name><affiliation><nlm:aff id="af3-ijms-14-23941">Department of Chemistry, Science College, AN-Najah National University, P.O. Box 7, Nablus, Palestine; E-Mail:<email>suleimanshtaya@najah.edu</email></nlm:aff></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">PMC</idno><idno type="pmid">24351867</idno><idno type="pmc">3876087</idno><idno type="url">http://www.ncbi.nlm.nih.gov/pmc/articles/PMC3876087</idno><idno type="RBID">PMC:3876087</idno><idno type="doi">10.3390/ijms141223941</idno><date when="2013">2013</date><idno type="wicri:Area/Pmc/Corpus">000425</idno><idno type="wicri:explorRef" wicri:stream="Pmc" wicri:step="Corpus" wicri:corpus="PMC">000425</idno><idno type="wicri:Area/Pmc/Curation">000424</idno><idno type="wicri:explorRef" wicri:stream="Pmc" wicri:step="Curation">000424</idno><idno type="wicri:Area/Pmc/Checkpoint">000181</idno><idno type="wicri:explorRef" wicri:stream="Pmc" wicri:step="Checkpoint">000181</idno><idno type="wicri:Area/Ncbi/Merge">000286</idno><idno type="wicri:Area/Ncbi/Curation">000286</idno><idno type="wicri:Area/Ncbi/Checkpoint">000286</idno><idno type="wicri:Area/Main/Merge">000214</idno><idno type="wicri:Area/Main/Curation">000213</idno><idno type="wicri:Area/Main/Exploration">000213</idno></publicationStmt><sourceDesc><biblStruct><analytic><title xml:lang="en" level="a" type="main">One Step Synthesis of NiO Nanoparticles via Solid-State Thermal Decomposition at Low-Temperature of Novel <italic>Aqua</italic>(2,9-dimethyl-1,10-phenanthroline)NiCl<sub>2</sub> Complex</title><author><name sortKey="Barakat, Assem" sort="Barakat, Assem" uniqKey="Barakat A" first="Assem" last="Barakat">Assem Barakat</name><affiliation><nlm:aff id="af1-ijms-14-23941">Department of Chemistry, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi Arabia; E-Mail:<email>ambarakat@ksu.edu.sa</email></nlm:aff></affiliation></author><author><name sortKey="Al Noaimi, Mousa" sort="Al Noaimi, Mousa" uniqKey="Al Noaimi M" first="Mousa" last="Al-Noaimi">Mousa Al-Noaimi</name><affiliation><nlm:aff id="af2-ijms-14-23941">Department of Chemistry, Hashemite University, Zarqa 13115, Jordan; E-Mail:<email>manoaimi@hu.edu.jo</email></nlm:aff></affiliation></author><author><name sortKey="Suleiman, Mohammed" sort="Suleiman, Mohammed" uniqKey="Suleiman M" first="Mohammed" last="Suleiman">Mohammed Suleiman</name><affiliation><nlm:aff id="af3-ijms-14-23941">Department of Chemistry, Science College, AN-Najah National University, P.O. Box 7, Nablus, Palestine; E-Mail:<email>suleimanshtaya@najah.edu</email></nlm:aff></affiliation></author><author><name sortKey="Aldwayyan, Abdullah S" sort="Aldwayyan, Abdullah S" uniqKey="Aldwayyan A" first="Abdullah S." last="Aldwayyan">Abdullah S. Aldwayyan</name><affiliation><nlm:aff id="af4-ijms-14-23941">Department of Physics and Astronomy, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi Arabia; E-Mail:<email>dwayyan@ksu.edu.sa</email></nlm:aff></affiliation></author><author><name sortKey="Hammouti, Belkheir" sort="Hammouti, Belkheir" uniqKey="Hammouti B" first="Belkheir" last="Hammouti">Belkheir Hammouti</name><affiliation><nlm:aff id="af5-ijms-14-23941">Laboratoire de Chimie Appliquée et Environnement, LCAE-URAC18, Faculity of Science, University Mohammed Premier, Oujda 60000, Morocco; E-Mail:<email>hammoutib@gmail.com</email></nlm:aff></affiliation></author><author><name sortKey="Ben Hadda, Taibi" sort="Ben Hadda, Taibi" uniqKey="Ben Hadda T" first="Taibi" last="Ben Hadda">Taibi Ben Hadda</name><affiliation><nlm:aff id="af6-ijms-14-23941">Lab of Chemical Material, FSO, University Mohammed Premier, Oujda 60000, Morocco; E-Mail:<email>taibi.ben.hadda@gmail.com</email></nlm:aff></affiliation></author><author><name sortKey="Haddad, Salim F" sort="Haddad, Salim F" uniqKey="Haddad S" first="Salim F." last="Haddad">Salim F. Haddad</name><affiliation><nlm:aff id="af7-ijms-14-23941">Department of Chemistry, the University of Jordan, Amman 11942, Jordan; E-Mail:<email>hadsal2003@yahoo.com</email></nlm:aff></affiliation></author><author><name sortKey="Boshaala, Ahmed" sort="Boshaala, Ahmed" uniqKey="Boshaala A" first="Ahmed" last="Boshaala">Ahmed Boshaala</name><affiliation><nlm:aff id="af8-ijms-14-23941">Department of Chemistry, Faculty of Science, Benghazi University, P.O. Box 1308, Benghazi 5341, Libya; E-Mail:<email>ahmedboshaala@yahoo.co.uk</email></nlm:aff></affiliation></author><author><name sortKey="Warad, Ismail" sort="Warad, Ismail" uniqKey="Warad I" first="Ismail" last="Warad">Ismail Warad</name><affiliation><nlm:aff id="af3-ijms-14-23941">Department of Chemistry, Science College, AN-Najah National University, P.O. Box 7, Nablus, Palestine; E-Mail:<email>suleimanshtaya@najah.edu</email></nlm:aff></affiliation></author></analytic><series><title level="j">International Journal of Molecular Sciences</title><idno type="eISSN">1422-0067</idno><imprint><date when="2013">2013</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><p>[NiCl<sub>2</sub>(C<sub>14</sub>H<sub>12</sub>N<sub>2</sub>)(H<sub>2</sub>O)] complex has been synthesized from nickel chloride hexahydrate (NiCl<sub>2</sub>·6H<sub>2</sub>O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as <italic>N</italic>,<italic>N</italic>-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired complex, subjected to thermal decomposition at low temperature of 400 ºC in an open atmosphere, revealed a novel and facile synthesis of pure NiO nanoparticles with uniform spherical particle; the structure of the NiO nanoparticles product was elucidated on the basis of Fourier transform infrared (FT-IR), UV-vis spectroscopy, TG/DTA, XRD, scanning electron microscopy (SEM), energy-dispersive X-ray spectrometry (EDXS) and transmission electron microscopy (TEM).</p></div></front><back><div1 type="bibliography"><listBibl><biblStruct><analytic><author><name sortKey="Wei, W" uniqKey="Wei W">W. Wei</name></author><author><name sortKey="Jiang, X" uniqKey="Jiang X">X. Jiang</name></author><author><name sortKey="Lu, L" uniqKey="Lu L">L. Lu</name></author><author><name sortKey="Yang, X" uniqKey="Yang X">X. 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Sheldrick</name></author></analytic></biblStruct></listBibl></div1></back></TEI><affiliations><list></list><tree><noCountry><name sortKey="Al Noaimi, Mousa" sort="Al Noaimi, Mousa" uniqKey="Al Noaimi M" first="Mousa" last="Al-Noaimi">Mousa Al-Noaimi</name><name sortKey="Aldwayyan, Abdullah S" sort="Aldwayyan, Abdullah S" uniqKey="Aldwayyan A" first="Abdullah S." last="Aldwayyan">Abdullah S. Aldwayyan</name><name sortKey="Barakat, Assem" sort="Barakat, Assem" uniqKey="Barakat A" first="Assem" last="Barakat">Assem Barakat</name><name sortKey="Ben Hadda, Taibi" sort="Ben Hadda, Taibi" uniqKey="Ben Hadda T" first="Taibi" last="Ben Hadda">Taibi Ben Hadda</name><name sortKey="Boshaala, Ahmed" sort="Boshaala, Ahmed" uniqKey="Boshaala A" first="Ahmed" last="Boshaala">Ahmed Boshaala</name><name sortKey="Haddad, Salim F" sort="Haddad, Salim F" uniqKey="Haddad S" first="Salim F." last="Haddad">Salim F. Haddad</name><name sortKey="Hammouti, Belkheir" sort="Hammouti, Belkheir" uniqKey="Hammouti B" first="Belkheir" last="Hammouti">Belkheir Hammouti</name><name sortKey="Suleiman, Mohammed" sort="Suleiman, Mohammed" uniqKey="Suleiman M" first="Mohammed" last="Suleiman">Mohammed Suleiman</name><name sortKey="Warad, Ismail" sort="Warad, Ismail" uniqKey="Warad I" first="Ismail" last="Warad">Ismail Warad</name></noCountry></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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